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Mössbauer spectroscopy : principles and applications / Alfred Maddock.

By: Contributor(s): Series: Horwood chemical science seriesPublisher: Chichester, England : Horwood Publishing, 1997Copyright date: ©1997Description: 1 online resource (273 pages) : illustrationsContent type:
  • text
Media type:
  • computer
Carrier type:
  • online resource
ISBN:
  • 9781782420606
  • 1782420606
Subject(s): Genre/Form: Additional physical formats: Print version:: Mössbauer spectroscopy : principles and applications.LOC classification:
  • QD96.M6 .M333 1997eb
Online resources:
Contents:
Front Cover; Mössbauer Spectroscopy Principles and Applications; Copyright Page; Table of Contents; Chapter 1. Basis of Mössbauer Spectroscopy; 1.1 RESONANCE ABSORPTION AND SCATTERING; 1.2 THE MöSSBAUER EFFECT; 1.3 INTERACTION OF NUCLEUS WITH ORBITAL ELECTRONS; 1 4 INTERACTION WITH THE ELECTRIC FIELD; 1.5 INTERACTION OF NUCLEUS WITH A MAGNETIC FIELD; 1.6 COMBINED MAGNETIC AND QUADRUPOLE INTERACTIONS; References for Chapter 1; Acknowledgements; Chapter 20. Practical aspects of Mössbauer Spectroscopy; 2.1 GENERAL NATURE OF TECHNIQUE; 2.2 SOURCES; 2.3 DETECTORS.
2.4 DOPPLER MODULATION OF PHOTON ENERGY2.5 CALIBRATION; 2 6 THE ABSORBER; 2.7 CRYOSTATS; 2.8 TREATMENT OF THE DATA; References; Chapter 3. Further consideration of principles; 3.1 INTENSITIES AND ANGULAR DISTRIBUTIONS; 3.2 INTENSITIES; 3.3 ANGULAR DEPENDENCE; 3.4 DEPARTURES FROM CALCULATED VALUES; 3.5 THE ELECTRIC FIELD GRADIENT; References; Acknowledgements; Chapter 4. Mössbauer Spectroscopy in Tin Chemistry; 4.1 MöSSBAUER SPECTRA OF MAIN GROUP ELEMENTS; 4.2 NUCLEAR ASPECTS OF TIN MöSSBAUER SPECTROSCOPY; 4.3 GENERAL FEATURES OF TIN MOSSBAUER SPECTRA; 4.4 ISOMER SHIFTS IN TIN(IV) COMPOUNDS.
4.5 ISOMER SHIFTS IN TIN(II) COMPOUNDS4.6. QUADRUPOLE SPLITTING IN TIN COMPOUNDS; 4.7 THE RECOIL FREE FRACTION; 4.8 SPECTRA IN A MATRIX; Acknowledgments; Chapter 5. Mössbauer Spectroscopy of Iron; 5.1 MöSSBAUER SPECTROSCOPY OF TRANSITION ELEMENTS; 5.2 NUCLEAR CONSIDERATIONS WITH 5 7Fe; 5.3 GENERAL FEATURES OF IRON MöSSBAUER SPECTRA; 5.4 HIGH SPIN IRON COMPOUNDS; 5.5 LOW SPIN IRON COMPOUNDS; 5.6 SIMPLE APPLICATIONS; 5.7 IRON IN HIGH OXIDATION STATES; 5.8. IRON IN UNUSUAL SPIN STATES; 5.9 FIVE COORDINATE IRON COMPLEXES; Acknowledgements; Chapter 6. Further consideration of magnetic effects.
6.1 HYPERFINE MAGNETIC FIELDS6.2 ORDERING IN MAGNETIC SOLIDS; 6.3 RELAXATION EFFECTS; 6.4. MAGNETIC SPECTRA FROM PARAMAGNETIC SOLIDS; 6.5 MAGNETICALLY ORDERED SYSTEMS; 6 6 MAGNETIC DIMENSIONALITY; 6.7 MAGNETIC PHASE CHANGES; Acknowledgements; Chapter 7. Further Features of Iron Spectra; 7.1 OXIDES AND HYDROXIDES; 7.2 SPINELS AND MIXED OXIDES; 7.3 LOW OXIDATION STATE COMPOUNDS; 7.4 MIXED VALENCE COMPOUNDS: DELOCALISATION; 7.5 SPIN CROSS-OVER; 7.6 IRON SPECIES IN SOLUTION, ON ADSORBENTS AND IN MATRICES; Acknowledgements; Chpter 8. CEMS and Applications in Mineralogy and Biochemistry.
8.1 CONVERSON ELECTRON MöSSBAUER SPECTROSCOPY, (CEMS)8.2 REACTIONS IN THE SOLID STATE; 8.3 APPLICATIONS TO MINERALOGY AND PETROLOGY; 8.4 AMORPHOUS MATERIALS; 8 5 APPLICATIONS IN BIOCHEMISTRY AND MEDICINE; 8.6 HAEM PROTEINS AND RELATED COMPOUNDS; 8.7 THE IRON-SULPHUR PROTEINS; 8.8 POROTEIN DTNAMICS; 8.9 MAGNETITE AND OTHER IRON COMPOUNDS IN ORGANISMS; Acknowledgements; Chpater 9. Mössbauer Spectroscopy of Elements Other Than Iron and Tin; 9.1 MAIN GROUP ELEMENTS; 9.2 OTHER TRANSITION ELEMENTS; 9.3 RARE EARTHS AND ACTINIDES; Acknowledgements; Chapter 10. Mössbauer Emission Spectroscopy.
Summary: Mossbauer spectroscopy has proved itself a versatile technique, finding applications in diverse areas of science and industry. Starting from physics and chemistry it spread into biochemistry, mineralogy, biochemistry, corrosion science, geochemistry and archaeology, with applications in industrial and scientific research. The author aims to help advanced university students, professionals and research workers who ask the question "what's in it for us?". After a concise account of experimental techniques, he emphasizes those applications in which there are few, if any, alternative ways of obtaining the same information about electron fields and the nuclei. He explains areas of industrial interest, including the important applications related to tin and iron on which there is much activity in research and development, and interprets the extension of Mossbauer techniques to main group, transitional and other suitable elements. Attention is paid to factors which may lead to misinterpretation of spectra and another chapter covers the complexities of interpreting emission spectra. Discusses the appearance of Mossbauer spectroscopy in biochemistry, mineralogy, biochemistry, corrosion science, geochemistry and archaeology, with applications in industrial and scientific researchEmphasizes the applications in which there are few, if any, alternative ways of obtaining the same information about electron fields and the nucleiAttention is paid to the complexities of interpreting emission spectra and the factors which may lead to misinterpretation of spectra.
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Includes bibliographical references at the end of each chapters and index.

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Mossbauer spectroscopy has proved itself a versatile technique, finding applications in diverse areas of science and industry. Starting from physics and chemistry it spread into biochemistry, mineralogy, biochemistry, corrosion science, geochemistry and archaeology, with applications in industrial and scientific research. The author aims to help advanced university students, professionals and research workers who ask the question "what's in it for us?". After a concise account of experimental techniques, he emphasizes those applications in which there are few, if any, alternative ways of obtaining the same information about electron fields and the nuclei. He explains areas of industrial interest, including the important applications related to tin and iron on which there is much activity in research and development, and interprets the extension of Mossbauer techniques to main group, transitional and other suitable elements. Attention is paid to factors which may lead to misinterpretation of spectra and another chapter covers the complexities of interpreting emission spectra. Discusses the appearance of Mossbauer spectroscopy in biochemistry, mineralogy, biochemistry, corrosion science, geochemistry and archaeology, with applications in industrial and scientific researchEmphasizes the applications in which there are few, if any, alternative ways of obtaining the same information about electron fields and the nucleiAttention is paid to the complexities of interpreting emission spectra and the factors which may lead to misinterpretation of spectra.

Front Cover; Mössbauer Spectroscopy Principles and Applications; Copyright Page; Table of Contents; Chapter 1. Basis of Mössbauer Spectroscopy; 1.1 RESONANCE ABSORPTION AND SCATTERING; 1.2 THE MöSSBAUER EFFECT; 1.3 INTERACTION OF NUCLEUS WITH ORBITAL ELECTRONS; 1 4 INTERACTION WITH THE ELECTRIC FIELD; 1.5 INTERACTION OF NUCLEUS WITH A MAGNETIC FIELD; 1.6 COMBINED MAGNETIC AND QUADRUPOLE INTERACTIONS; References for Chapter 1; Acknowledgements; Chapter 20. Practical aspects of Mössbauer Spectroscopy; 2.1 GENERAL NATURE OF TECHNIQUE; 2.2 SOURCES; 2.3 DETECTORS.

2.4 DOPPLER MODULATION OF PHOTON ENERGY2.5 CALIBRATION; 2 6 THE ABSORBER; 2.7 CRYOSTATS; 2.8 TREATMENT OF THE DATA; References; Chapter 3. Further consideration of principles; 3.1 INTENSITIES AND ANGULAR DISTRIBUTIONS; 3.2 INTENSITIES; 3.3 ANGULAR DEPENDENCE; 3.4 DEPARTURES FROM CALCULATED VALUES; 3.5 THE ELECTRIC FIELD GRADIENT; References; Acknowledgements; Chapter 4. Mössbauer Spectroscopy in Tin Chemistry; 4.1 MöSSBAUER SPECTRA OF MAIN GROUP ELEMENTS; 4.2 NUCLEAR ASPECTS OF TIN MöSSBAUER SPECTROSCOPY; 4.3 GENERAL FEATURES OF TIN MOSSBAUER SPECTRA; 4.4 ISOMER SHIFTS IN TIN(IV) COMPOUNDS.

4.5 ISOMER SHIFTS IN TIN(II) COMPOUNDS4.6. QUADRUPOLE SPLITTING IN TIN COMPOUNDS; 4.7 THE RECOIL FREE FRACTION; 4.8 SPECTRA IN A MATRIX; Acknowledgments; Chapter 5. Mössbauer Spectroscopy of Iron; 5.1 MöSSBAUER SPECTROSCOPY OF TRANSITION ELEMENTS; 5.2 NUCLEAR CONSIDERATIONS WITH 5 7Fe; 5.3 GENERAL FEATURES OF IRON MöSSBAUER SPECTRA; 5.4 HIGH SPIN IRON COMPOUNDS; 5.5 LOW SPIN IRON COMPOUNDS; 5.6 SIMPLE APPLICATIONS; 5.7 IRON IN HIGH OXIDATION STATES; 5.8. IRON IN UNUSUAL SPIN STATES; 5.9 FIVE COORDINATE IRON COMPLEXES; Acknowledgements; Chapter 6. Further consideration of magnetic effects.

6.1 HYPERFINE MAGNETIC FIELDS6.2 ORDERING IN MAGNETIC SOLIDS; 6.3 RELAXATION EFFECTS; 6.4. MAGNETIC SPECTRA FROM PARAMAGNETIC SOLIDS; 6.5 MAGNETICALLY ORDERED SYSTEMS; 6 6 MAGNETIC DIMENSIONALITY; 6.7 MAGNETIC PHASE CHANGES; Acknowledgements; Chapter 7. Further Features of Iron Spectra; 7.1 OXIDES AND HYDROXIDES; 7.2 SPINELS AND MIXED OXIDES; 7.3 LOW OXIDATION STATE COMPOUNDS; 7.4 MIXED VALENCE COMPOUNDS: DELOCALISATION; 7.5 SPIN CROSS-OVER; 7.6 IRON SPECIES IN SOLUTION, ON ADSORBENTS AND IN MATRICES; Acknowledgements; Chpter 8. CEMS and Applications in Mineralogy and Biochemistry.

8.1 CONVERSON ELECTRON MöSSBAUER SPECTROSCOPY, (CEMS)8.2 REACTIONS IN THE SOLID STATE; 8.3 APPLICATIONS TO MINERALOGY AND PETROLOGY; 8.4 AMORPHOUS MATERIALS; 8 5 APPLICATIONS IN BIOCHEMISTRY AND MEDICINE; 8.6 HAEM PROTEINS AND RELATED COMPOUNDS; 8.7 THE IRON-SULPHUR PROTEINS; 8.8 POROTEIN DTNAMICS; 8.9 MAGNETITE AND OTHER IRON COMPOUNDS IN ORGANISMS; Acknowledgements; Chpater 9. Mössbauer Spectroscopy of Elements Other Than Iron and Tin; 9.1 MAIN GROUP ELEMENTS; 9.2 OTHER TRANSITION ELEMENTS; 9.3 RARE EARTHS AND ACTINIDES; Acknowledgements; Chapter 10. Mössbauer Emission Spectroscopy.

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